Journal Highlight: Determination of free fatty acids in edible oils by 1H NMR spectroscopy

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  • Published: Jan 7, 2013
  • Author: spectroscopyNOW
  • Channels: NMR Knowledge Base
thumbnail image: Journal Highlight: Determination of free fatty acids in edible oils by <sup>1</sup>H NMR spectroscopy

Determination of free fatty acids in edible oils by 1H NMR spectroscopy

Lipid Technology, 2012, 24, 279-281
Christina Skiera, Panagiotis Steliopoulos, Thomas Kuballa, Ulrike Holzgrabe, Bernd Diehl

A novel proton NMR assay for the determination of free fatty acids in edible oils is a suitable alternative to the acid value method.

Abstract: Here we describe a novel 1H NMR assay for the determination of free fatty acids (FFAs) in edible oils. The analytical performance of the NMR assay is similar to that of the commonly used acid value (AV) method. A total of 120 edible oil samples were analysed by both approaches. Except for pumpkin seed oil, showing slight deviations, there was a good compliance between the results obtained from the two methods.

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