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Journal Highlight: Establishing the transitory existence of amorphous phases in crystallization pathways by the CLASSIC NMR technique

Date: Nov 26, 2018

Author: spectroscopyNOW

CLASSIC NMR (Combined Liquid‐ And Solid‐State In‐situ Crystallization NMR) has been used to reveal the transitory existence of amorphous phases during crystallization processes, demonstrating with DL‐menthol and L‐menthol.

Read More thumbnail image: Journal Highlight Establishing the transitory existence of amorphous phases in crystallization pathways by the CLASSIC NMR technique

CryoEM to usurp NMR? Small molecules succumb

Date: Nov 15, 2018

Author: David Bradley

Nuclear magnetic resonance (NMR) spectroscopy has been an invaluable tool for fifty years allowing chemists and others to figure out the structures of a vast range of molecules based on inferring connectivity between the atoms particular in small organic molecules. Now, that relative upstart technique electron cryo-microscopy (cryoEM) has been used to provide routine and unambiguous structural determination of small organic molecules that one might see as augmenting NMR studies and perhaps even going one...

Read More thumbnail image: CryoEM to usurp NMR Small molecules succumb

Flexible, stable: Against cancer

Date: Nov 1, 2018

Author: David Bradley

Various techniques have been used in studies that show how linking therapeutically active molecules to specific antibodies can help them target disease sites, specifically in cancer, and so minimize side effects.

Read More thumbnail image: Flexible stable Against cancer

Journal Highlight: Application of nuclear magnetic resonance permeability models in tight reservoirs

Date: Oct 29, 2018

Author: spectroscopyNOW

Existing models for NMR‐based estimates of tight reservoir permeability have been discussed and applied to tight reservoirs from North America, Asia, and Europe to help choose the best NMR permeability estimation model.

Read More thumbnail image: Journal Highlight Application of nuclear magnetic resonance permeability models in tight reservoirs

New cat on the block: NMR clues

Date: Oct 15, 2018

Author: David Bradley

Polymers synthesized using electropolymerization are attracting attention once again in the world of catalytic research. One of the first pairings of nuclear magnetic resonance (NMR) spectroscopy and electrochemical tests reveals the details.

Read More thumbnail image: New cat on the block NMR clues

Journal Highlight: Extra‐large NMR spectroscopy (XLSY)

Date: Oct 1, 2018

Author: spectroscopyNOW

eXtra Large NMR SpectroscopY (XLSY)  has been developed for experimental data collection, reconstruction and handling of very large NMR spectra by a combination of radial and non‐uniform sampling, a new processing algorithm and rigorous statistical validation.

Read More thumbnail image: Journal Highlight Extralarge NMR spectroscopy XLSY

Up-converting radio: NMR sees the light

Date: Oct 1, 2018

Author: David Bradley

Up-converting radio-frequency signals to the optical range opens up a new , more sensitive way to use nuclear magnetic resonance (NMR) spectroscopy, according to an international team led by Kazuyuki Takeda of Kyoto University and Koji Usami of the University of Tokyo.

Read More thumbnail image: Up-converting radio NMR sees the light

Bactericidal polymers: Phosphorus NMR links up activity

Date: Sep 15, 2018

Author: David Bradley

Researchers in Canada have used phosphorus-31 nuclear magnetic resonance (NMR) spectroscopy to study hydrophilic phosphonium polymers that have surprising antibacterial activity and selectivity.

Read More thumbnail image: Bactericidal polymers Phosphorus NMR links up activity

Journal Highlight: Important issues in plant tissues analyses by HR‐MAS NMR

Date: Sep 3, 2018

Author: spectroscopyNOW

A study of the method variables in the HR‐MAS NMR analysis of plant tissues has highlighted the need for standardised sample preparation and instrumental setup protocols in order to achieve high reproducibility and reliable data.

Read More thumbnail image: Journal Highlight Important issues in plant tissues analyses by HRMAS NMR

Autophagy: NMR and MS reveal tumour regrowth mechanism

Date: Sep 1, 2018

Author: David Bradley

The combined forces of nuclear magnetic resonance (NMR) spectroscopy and mass spectrometry have been used in research that shows how cell metabolism affects the ability of cells to undergo a survival program called autophagy during cancer chemotherapy allowing a tumour to regrow.

Read More thumbnail image: Autophagy NMR and MS reveal tumour regrowth mechanism
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